N,N-Bis(2-hydroxy)-p-phenylenediamine sulfate

CAS Number54381-16-7
Molecular FormulaC10H18N2O6S
Molecular Weight294.33
InChI KeyKMCFMEHSEWDYKG-UHFFFAOYSA-N
Synonyms
  • 54381-16-7
  • N,N-Bis(2-hydroxy)-p-phenylenediamine sulfate
  • N,N-BIS(2-HYDROXYETHYL)-4-PHENYLENEDIAMINE SULPHATE
  • N,N-Bis(2-hydroxyethyl)-4-phenylenediaminesulfate
  • N,N-BIS(2-HYDROXYETHYL)-4-PHENYLENEDIAMINESULPHATE
  • 2,2'-((4-Aminophenyl)azanediyl)diethanol sulfate
  • N,N-Bis(2-hydroxyethyl)-p-phenylenediamine sulphate
  • N,N-Bis(2-hydroxyethyl)-1,4-phenylenediamine sulfate
  • N,N-Bis(2-hydroxyethyl)-p-phenylenediamine sulfate
  • Ro 371
  • 2,2'-[(4-Aminophenyl)imino]bisethanol sulfate
  • 3X5A8DP6HC
  • (p-Ammoniophenyl)bis(2-hydroxyethyl)ammonium sulphate
  • 2-[4-amino-N-(2-hydroxyethyl)anilino]ethanol;sulfuric acid
  • Ethanol, 2,2'-((4-aminophenyl)imino)bis-, sulfate (1:1) (salt)
  • MFCD00013177
  • Ethanol, 2,2'-((4-aminophenyl)imino)bis-, sulfate (salt)
  • Ethanol, 2,2'-[(4-aminophenyl)imino]bis-, sulfate (1:1) (salt)
  • 2,2'-((4-Aminophenyl)imino)bisethanol sulfate
  • CCRIS 7702
  • EINECS 259-134-5
  • UNII-3X5A8DP6HC
  • T 32
  • 2,2-[(4-Aminophenyl)azanediyl]diethanol sulfate
  • 4-Amino-N,N-di(beta-hydroxyethyl)aniline sulfate
  • 2,2'-((4-Aminophenyl)imino)bis(ethanol) sulfate
  • N,N-Bis-(2-hydroxyethyl)-p-phenylenediamine sulfate
  • 2,2'-((4-Aminophenyl)imino)bisethanol sulfate (salt)
  • N,N-Bis(beta-hydroxyethyl)-p-phenylenediamine sulfate
  • N,N-Bis-2-hydroxyethyl-p-fenylendiamin siran [Czech]

Applications:

HPLC Method for Analysis of N,N-Bis (2-hydroxy)-p-phenylenediamine on Primesep 100 Column

November 29, 2023

HPLC Method for Analysis of N,N-Bis (2-hydroxy)-p-phenylenediamine on Primesep 100 by SIELC Technologies

HPLC Method for Analysis of N,N-Bis(2-hydroxy)-p-phenylenediamine on Primesep 100 Column by SIELC Technologies


 High Performance Liquid Chromatography (HPLC) Method for Analysis of N,N-Bis(2-hydroxy)-p-phenylenediamine

N,N-Bis(2-hydroxyethyl)-p-phenylenediamine (often abbreviated as N,N-Bis(2-hydroxyethyl)-PPD) is a chemical compound that is a derivative of p-phenylenediamine (PPD), a common ingredient in hair dyes.

The N,N-Bis(2-hydroxyethyl)-p-phenylenediamine be retained and analyzed using a Primesep 100 mixed-mode stationary phase column. The analysis employs an isocratic method with a simple mobile phase comprising water, acetonitrile (MeCN), and sulfuric acid as a buffer. This method allows for detection using UV at 210 nm

ColumnPrimesep 100, 4.6 x 150 mm, 5 µm, 100 A
Mobile PhaseMeCN/H2O – 30/70%
BufferH2SO4 -0.2%
Flow Rate1.0 ml/min
DetectionUV 210 nm
SamplesN,N-Bis(2-hydroxy)-p-phenylenediamine (0.7 mg/mL)
Injection volume3 µl

Class of Compounds
Aromatic amines
Analyzing CompoundsN,N-Bis(2-hydroxy)-p-phenylenediamine sulfate

Application Column

Primesep 100

Column Diameter: 4.6 mm
Column Length: 150 mm
Particle Size: 5 µm
Pore Size: 100 A

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Application Analytes:
N,N-Bis(2-hydroxy)-p-phenylenediamine sulfate

Application Detection:
UV Detection
SIELC Technologies usually develops more than one method for each compound. Therefore, this particular method may not be the best available method from our portfolio for your specific application. Before you decide to implement this method in your research, please send us an email to research@sielc.com so we can ensure you get optimal results for your compound/s of interest.

HPLC Method for Separation of a Mixture of Resorcinol, N,N-Bis (2-hydroxy)-p-phenylenediamine, p-Phenylenediamine and 1-Naphthol on Primesep 100 Column

November 29, 2023

HPLC Method for Analysis of Resorcinol, N,N-Bis (2-hydroxy)-p-phenylenediamine, p-Phenylenediamine and 1-Naphthol on Primesep 100 by SIELC Technologies

HPLC Method for Analysis of Resorcinol, N,N-Bis(2-hydroxy)-p-phenylenediamine, p-Phenylenediamine and 1-Naphtholon Primesep 100 Column by SIELC Technologies


 High Performance Liquid Chromatography (HPLC) Method for Analysis of  Resorcinol, N,N-Bis(2-hydroxy)-p-phenylenediamine, p-Phenylenediamine and 1-Naphthol

Resorcinol – a chemical compound with the formula C6H4(OH)2. It is a dihydroxybenzene used in various applications, including the production of resins and as a topical antiseptic.

N,N-Bis(2-hydroxyethyl)p-phenylenediamine – a compound used in the manufacture of hair dyes and related products.

p-Phenylenediamine – commonly known as PPD, it’s used in hair dyes and black rubber products.

1-Naphthol – a crystalline compound with the formula C10H7OH. It’s used in the synthesis of dyes and perfumes.

All compounds can be retained, separated, and analyzed using a Primesep 100 mixed-mode stationary phase column. The analysis employs an isocratic method with a simple mobile phase comprising water, acetonitrile (MeCN), and sulfuric acid as a buffer. This method allows for detection using UV at 210 nm

ColumnPrimesep 100, 4.6 x 150 mm, 5 µm, 100 A
Mobile PhaseMeCN/H2O – 30/70%
BufferH2SO4 -0.2%
Flow Rate1.0 ml/min
DetectionUV 210 nm
SamplesN,N-Bis(2-hydroxy)-p-phenylenediamine (0.7 mg/mL)
p-Phenylenediamine (1.3 mg/mL)
1-Naphthol (0.18 mg/mL)
Resorcinol (0.28 mg/mL)
Injection volume3 µl

Class of Compounds
Phenols, Aromatic amines
Analyzing CompoundsResorcinol, 1-Naphthol, N,N-Bis(2-hydroxy)-p-phenylenediamine sulfate, m-Phenylenediamine

Application Column

Primesep 100

Column Diameter: 4.6 mm
Column Length: 150 mm
Particle Size: 5 µm
Pore Size: 100 A

Add to cart
Application Analytes:
1-Naphthol
N,N-Bis(2-hydroxy)-p-phenylenediamine sulfate
Resorcinol
m-Phenylenediamine

Application Detection:
UV Detection
SIELC Technologies usually develops more than one method for each compound. Therefore, this particular method may not be the best available method from our portfolio for your specific application. Before you decide to implement this method in your research, please send us an email to research@sielc.com so we can ensure you get optimal results for your compound/s of interest.