Allyl bromide

Allyl bromide structural formula

CAS Number106-95-6
Molecular FormulaC3H5Br
Molecular Weight120.977
InChI KeyBHELZAPQIKSEDF-UHFFFAOYSA-N
LogP1.79
Synonyms
  • Allyl bromide
  • 3-Bromoprop-1-ene
  • 1-Propene, 3-bromo-
  • 106-95-6
  • 1-Propene, 3-bromo-
  • 1-BROM-2-PROPEN
  • 1-Bromo-2-propene
  • 2-Propenyl bromide
  • 3-Bromo-1-propene
  • 3-bromopropene
  • 3-bromopropeno
  • 3-Bromopropylene
  • 3-Brompropen
  • NSC 7596
  • PROPENE, 3-BROMO-
  • UN 1099
  • BRN 0605308
  • Bromallylene
  • EINECS 203-446-6
  • UNII-FXQ8X2F74Z

Applications:

HPLC Determination of Allyl Bromide on Newcrom R1 Column

November 7, 2019

HPLC Method for Allyl bromide on Newcrom R1 by SIELC Technologies

HPLC Determination of Allyl Bromide on Newcrom R1 Column_1196

High Performance Liquid Chromatography (HPLC) Method for Analysis of Allyl bromide.

Allyl Bromide is an organic halide with C3H5Br chemical formula. It is an alkylating agent typically found in synthesis of polymers, pharmaceuticals, perfumes, and more. Often, it is used as starting material in organic synthesis. Physically, it is a colorless liquid that occasionally presents more yellow.  It is toxic to people by skin absorption, irritable to eyes and respiratory system.

Allyl bromide can be retained and analyzed using the Newcrom R1 stationary phase column. The analysis utilizes an isocratic method with a simple mobile phase consisting of water and acetonitrile (MeCN) with a triethanolamine buffer. Detection is performed using UV.

Condition
Column Newcrom R1, 4.6 x 150 mm, 5 µm, 100 A, dual ended
Mobile Phase MeCN/H2O – 60/40%
Flow Rate 1.0 ml/min
Detection UV 210 nm

 

Description
Class of Compounds
 Organic halide, Hydrophobic, Ionizable
Analyzing Compounds Allyl bromide

 

Application Column

Newcrom R1

Column Diameter: 4.6 mm
Column Length: 150 mm
Particle Size: 5 µm
Pore Size: 100 A
Column options: dual ended

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Application Analytes:
Allyl bromide
Application Detection:
UV Detection
SIELC Technologies usually develops more than one method for each compound. Therefore, this particular method may not be the best available method from our portfolio for your specific application. Before you decide to implement this method in your research, please send us an email to research@sielc.com so we can ensure you get optimal results for your compound/s of interest.

Separation of Allyl bromide on Newcrom R1 HPLC column

May 16, 2018
Separation of Allyl bromide on Newcrom R1 HPLC column

Allyl bromide can be analyzed by this reverse phase (RP) HPLC method with simple conditions. The mobile phase contains an acetonitrile (MeCN), water, and phosphoric acid. For Mass-Spec (MS) compatible applications the phosphoric acid needs to be replaced with formic acid. Smaller 3 µm particles columns available for fast UPLC applications. This liquid chromatography method is scalable and can be used for isolation impurities in preparative separation. It also suitable for pharmacokinetics.

Application Column

Newcrom R1

The Newcrom columns are a family of reverse-phase-based columns. Newcrom A, AH, B, and BH are all mixed-mode columns with either positive or negative ion-pairing groups attached to either short (25 Å) or long (100 Å) ligand chains. Newcrom R1 is a special reverse-phase column with low silanol activity.

Select options
Application Analytes:
Allyl bromide
SIELC Technologies usually develops more than one method for each compound. Therefore, this particular method may not be the best available method from our portfolio for your specific application. Before you decide to implement this method in your research, please send us an email to research@sielc.com so we can ensure you get optimal results for your compound/s of interest.