HPLC Method For Analysis Of 2,3-Dichlorobenzoic Anhydride on Primesep S2 Column

HPLC Method for 2,3-Dichlorobenzoic anhydride on Primesep S2 by SIELC Technologies

High Performance Liquid Chromatography (HPLC) Method for Analysis of 2,3-Dichlorobenzoic anhydride.

2,3-Dichlorobenzoic Anhydride is an impurity with the chemical formula C14H6Cl4O3. It is formed during the production of Lamotrigine, anticonvulsant used to treat epileptic seizures and Bipolar Disorder. Removing 2,3-Dichlorobenzoic Anhydride is paramount for maximizing Lamotrigine purity. It had no known uses outside of quality control. You can find detailed UV spectra of 2,3-Dichlorobenzoic anhydride and information about its various lambda maxima by visiting the following link.

2,3-Dichlorobenzoic anhydride can be retained and analyzed using the Primesep S2 stationary phase column. The analysis utilizes an isocratic method with a simple mobile phase consisting of acetonitrile (MeCN). Detection is performed using UV.

Condition
Column Primesep S2, 4.6 x 250 mm, 5 µm, 100 A, dual ended
Mobile Phase MeCN- 100%
Buffer No
Flow Rate 1.0 ml/min
Detection UV 210 nm

Description
Class of Compounds Anhydride
Analyzing Compounds 2,3-Dichlorobenzoic anhydride

Application Column

Primesep S2

Column Diameter: 4.6 mm
Column Length: 250 mm
Particle Size: 5 µm
Pore Size: 100 A
Column options: dual ended

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Application Analytes:
2,3-Dichlorobenzoic anhydride
Application Detection:
UV Detection
SIELC Technologies usually develops more than one method for each compound. Therefore, this particular method may not be the best available method from our portfolio for your specific application. Before you decide to implement this method in your research, please send us an email to research@sielc.com so we can ensure you get optimal results for your compound/s of interest.