Xylylenediamine

Xylylenediamine structural formula

CAS Number1477-55-0
Molecular FormulaC8H12N2
Molecular Weight136.198
InChI KeyFDLQZKYLHJJBHD-UHFFFAOYSA-N
LogP0.196
Synonyms
  • 1,3-Benzenedimethanamine
  • (1,3-Phenylene)dimethanamine
  • 1477-55-0
  • m-Xylylenediamine
  • 1,3-Benzenebis(methylamine)
  • 1,3-Bis(aminomethyl)benzene
  • 1,3-bis-Aminomethylbenzene
  • 1,3-Xylylenediamine
  • 3-(Aminomethyl)benzylamine
  • BENZENE, 1,3-DI(AMINOMETHYL)-
  • Epilink MX
  • m-(α,α'-Diamino)xylene
  • META-XYLENE DIAMINE
  • METAXYLYLENEDIANINE
  • m-fenilenbis(metilamina)
  • m-Phenylenbis(methylamin)
  • m-phenylenebis(methylamine)
  • m-Xylene α, α'-diamine
  • m-Xylene-α,α'-diamine
  • M-XYLYLENE DIAMINE
  • NSC 61568
  • α,α'-Diamino-m-xylene
  • α,α'-m-Xylenediamine
  • BRN 1099911
  • alpha,alpha'-Diamino-m-xylene
  • EINECS 216-032-5
  • m-Xylene-alpha,alpha'-diamine
  • 1,3-Bis-aminomethylbenzen
  • m-Xylylendiamin
  • UNII-1E84B9YLJD
  • 153326-45-5
  • 554432-83-6

Applications:

HPLC Method For Analysis of Xylylenediamine on BIST B+ Column

June 15, 2022

HPLC Method for Xylylenediamine, m-Xylylenediamine on BIST B+ by SIELC Technologies

High Performance Liquid Chromatography (HPLC) Method for Analysis of Xylylenediamine, m-Xylylenediamine.

m-Xylylenediamine (MXDA) is a popular curing agent used on epoxy resins with the chemical formula C8H12N2. When MXDA undergoes the Sommelet reaction, it results in a isophthalaldehyde. You can find detailed UV spectra of m-Xylylenediamine and information about its various lambda maxima by visiting the following link.

Using SIELC’s newly introduced BIST method, Xylylenediamine, m-Xylylenediamine, which protonates in water, can be retained on a positively-charged anion-exchange BIST B+ column. There are two keys to this retention method: 1) a multi-charged, negative buffer, such as Sulfuric acid (H2SO4), which acts as a bridge, linking the positively-charged MXDA analytes to the positively-charged column surface and 2) a mobile phase consisting mostly of organic solvent (such as MeCN) to minimize the formation of a solvation layer around the charged analytes. Using this new and unique analysis method, MXDA can be retained and UV detected at 210 nm.

Condition
Column BIST B+, 4.6 x 150 mm, 5 µm, 100 A, dual ended
Mobile Phase MeCN/H2O – 70/30%
Buffer H2SO4 – 0.2 %
Flow Rate 1.0 ml/min
Detection UV, 210 nm

 

Description
Class of Compounds
 Drug, Basic, Hydrophobic, Ionizable, Zwitterionic
Analyzing Compounds Xylylenediamine, m-Xylylenediamine

 

Application Column

BIST B+

Column Diameter: 4.6 mm
Column Length: 150 mm
Particle Size: 5 µm
Pore Size: 100 A
Column options: dual ended

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Application Analytes:
Xylylenediamine
m-Xylylenediamine
Application Detection:
UV Detection
SIELC Technologies usually develops more than one method for each compound. Therefore, this particular method may not be the best available method from our portfolio for your specific application. Before you decide to implement this method in your research, please send us an email to research@sielc.com so we can ensure you get optimal results for your compound/s of interest.

Analysis of m-Xylylenediamine (MXDA)

February 15, 2012

Condition
Column Primesep AP, 4.6×150 mm, 5 µm, 100A
Mobile Phase MeCN/H2O
Buffer H2SO4 – 0.2 %
Flow Rate 1.0 ml/min
Detection UV, 215 nm

 

Description
Class of Compounds
 Drug, Basic, Hydrophobic, Ionizable, Zwitterionic
Analyzing Compounds m-Xylylenediamine (MXDA)

 

Application Column

Primesep AP

The Primesep family of mixed-mode columns offers a wide variety of stationary phases, boasting unprecedented selectivity in the separation of a broad array of chemical compounds across multiple applications. Corresponding Primesep guard columns, available with all stationary phases, do not require holders. SIELC provides a method development service available to all customers. Inquire about our specially-tailored custom LC-phases for specific separations.

Select options
Application Analytes:
MXDA
Xylylenediamine
m-Xylylenediamine
SIELC Technologies usually develops more than one method for each compound. Therefore, this particular method may not be the best available method from our portfolio for your specific application. Before you decide to implement this method in your research, please send us an email to research@sielc.com so we can ensure you get optimal results for your compound/s of interest.