Tribenzylamine

Tribenzylamine structural formula

CAS Number620-40-6
Molecular FormulaC21H21N
Molecular Weight287.407
InChI KeyMXHTZQSKTCCMFG-UHFFFAOYSA-N
LogP4.84
Synonyms
  • Tribenzylamine
  • N,N-Dibenzyl-1-phenylmethanamine
  • Benzenemethanamine, N,N-bis(phenylmethyl)-
  • 620-40-6
  • EINECS 210-638-3

Applications:

HPLC Method for Analysis of Tribenzylamine in Copper Plating Bath Solution on Primesep B  Column

July 7, 2023

HPLC Method for Separation of Tribenzylamine on Primesep B by SIELC Technologies

Separation type: Liquid Chromatography Mixed-mode

HPLC Method for Analysis of Tribenzylamine in Copper Plating Bath Solution on Primesep B  Column
HPLC Method for Analysis of Tribenzylamine in Copper Plating Bath Solution on Primesep B  Column

Tribenzylamine (TBA) is an organic compound that falls under the class of triarylamines.

Tribenzylamine (TBA) is an organic compound that is sometimes used in the formulation of electrolyte solutions for copper plating. Copper plating is a process that involves the deposition of a layer of copper onto a substrate, and it requires an electrolyte solution to facilitate the transfer of copper ions to the substrate.

Tribenzylamine can act as a leveler or brightener in the copper plating process. Levelers and brighteners are additives used in plating baths to improve the appearance and properties of the plated surface. They can help to achieve a smoother, brighter, and more uniform finish by influencing the rate and distribution of metal ion deposition.

In a copper plating bath, tribenzylamine might be used alongside other components such as copper sulfate (the primary source of copper ions), sulfuric acid (which improves the conductivity of the bath and helps to control pH), and other additives that serve to fine-tune the properties of the plated layer.

It’s often used in organic chemistry as a reagent, particularly in the production of other complex organic compounds.

The Tribenzylamine can be retained and analyzed using a mixed-mode Primesep B, 4.6 x 150 mm, 5 µm, 100 A column. The mobile phase for this method consists of water, acetonitrile (MeCN), and Sulfuric acid, which serves as a buffer. This analytical method can be monitored using UV detection at 200 nm.

LOD was determined for this combination of instrument, method, and analyte, and it can vary from one laboratory to another even when the same general type of analysis is being performed.

High Performance Liquid Chromatography (HPLC) Method for Analysis of Tribenzylamine

Condition

ColumnPrimesep B, 4.6 x 150 mm, 5 µm, 100 A
Mobile PhaseMeCN -20%
BufferH2SO4 – 0.1%
Flow Rate1.0 ml/min
DetectionUV 200 nm
Peak Retention Time5.3 min
Sample concentration0.01 mg/ml
Injection volume10 µl
Sample diluentH2SO4 -10%, CuSO4– 4% in H2O
LOD10 ppb

Description

Class of CompoundsTriarylamines
Analyzing CompoundsTribenzylamine

Application Column

Primesep B

Column Diameter: 4.6 mm
Column Length: 150 mm
Particle Size: 5 µm
Pore Size: 100 A

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Application Analytes:
Tribenzylamine
SIELC Technologies usually develops more than one method for each compound. Therefore, this particular method may not be the best available method from our portfolio for your specific application. Before you decide to implement this method in your research, please send us an email to research@sielc.com so we can ensure you get optimal results for your compound/s of interest.

HPLC Method for Analysis of Tribenzylamine (TBA)  on Primesep B Column

July 6, 2023

HPLC Method for Separation of Tribenzylamine on Primesep B by SIELC Technologies

Separation type: Liquid Chromatography Mixed-mode

HPLC Method for Analysis of Tribenzylamine on Primesep B Column by SIELC Technologies
HPLC Method for Analysis of Tribenzylamine (TBA)  on Primesep B Colum

Tribenzylamine (TBA) is an organic compound that falls under the class of triarylamines.

Triarylamines are compounds containing an amine group (-NH2) attached to three aromatic groups (in this case, benzyl groups). In the case of tribenzylamine, the amine nitrogen is attached to three benzyl groups, which are phenyl (benzene) rings attached to a methylene (-CH2-) group.

So, tribenzylamine has the formula (C6H5CH2)3N, with the three benzyl groups making it a tertiary amine.

It’s often used in organic chemistry as a reagent, particularly in the production of other complex organic compounds.

The Tribenzylamine can be retained and analyzed using a mixed-mode Primesep B, 3.2 x 100 mm, 5 µm, 100 A column. The mobile phase for this method consists of water, acetonitrile (MeCN), and Sulfuric acid, which serves as a buffer. This analytical method can be monitored using UV detection at 200 nm.

High Performance Liquid Chromatography (HPLC) Method for Analysis of Tribenzylamine

Condition

ColumnPrimesep B, 3.2 x 100 mm, 5 µm, 100 A
Mobile PhaseMeCN -10%
BufferH2SO4 – 0.1%
Flow Rate0.5 ml/min
DetectionUV 200 nm

Description

Class of CompoundsTriarylamines
Analyzing CompoundsTribenzylamine

Application Column

Primesep B

Column Diameter: 3.2 mm
Column Length: 100 mm
Particle Size: 5 µm
Pore Size: 100 A

Add to cart
Application Analytes:
Tribenzylamine

Application Detection:
UV Detection
SIELC Technologies usually develops more than one method for each compound. Therefore, this particular method may not be the best available method from our portfolio for your specific application. Before you decide to implement this method in your research, please send us an email to research@sielc.com so we can ensure you get optimal results for your compound/s of interest.

HPLC Determination of Tribenzylamine on Primesep B Column

July 31, 2020


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Condition

Column Primesep B, 4.6×150 mm, 5 µm, 100A
Mobile Phase Gradient MeCN 20-40% , 10 min
Buffer AmFm pH 3.0- 40 mM
Flow Rate 1.0 ml/min
Detection UV, 260 nm, (MS-compatible mobile phase)

 

Description

Class of Compounds
Hydrophobic
Analyzing Compounds Tribenzylamine

 

Application Column

Primesep B

The Primesep family of mixed-mode columns offers a wide variety of stationary phases, boasting unprecedented selectivity in the separation of a broad array of chemical compounds across multiple applications. Corresponding Primesep guard columns, available with all stationary phases, do not require holders. SIELC provides a method development service available to all customers. Inquire about our specially-tailored custom LC-phases for specific separations.

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Application Analytes:
Tribenzylamine
SIELC Technologies usually develops more than one method for each compound. Therefore, this particular method may not be the best available method from our portfolio for your specific application. Before you decide to implement this method in your research, please send us an email to research@sielc.com so we can ensure you get optimal results for your compound/s of interest.

Separation of Tribenzylamine on Newcrom R1 HPLC column

February 16, 2018
Separation of Tribenzylamine on Newcrom C18 HPLC column

Tribenzylamine can be analyzed by this reverse phase (RP) HPLC method with simple conditions. The mobile phase contains an acetonitrile (MeCN), water, and phosphoric acid. For Mass-Spec (MS) compatible applications the phosphoric acid needs to be replaced with formic acid. Smaller 3 µm particles columns available for fast UPLC applications. This liquid chromatography method is scalable and can be used for isolation impurities in preparative separation. It also suitable for pharmacokinetics.

Application Column

Newcrom R1

The Newcrom columns are a family of reverse-phase-based columns. Newcrom A, AH, B, and BH are all mixed-mode columns with either positive or negative ion-pairing groups attached to either short (25 Å) or long (100 Å) ligand chains. Newcrom R1 is a special reverse-phase column with low silanol activity.

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Application Analytes:
Tribenzylamine
The result was obtained by a proprietary SIELC algorithm. It may deviate from the actual experimental data. The experimental data are available upon request. Contact us by e-mail: support@sielc.com or by phone: 847-229-2629.