Fluroxypyr-meptyl

Fluroxypyr-meptyl structural formula

CAS Number81406-37-3
Molecular FormulaC15H21Cl2FN2O3
Molecular Weight367.240
InChI KeyOLZQTUCTGLHFTQ-UHFFFAOYSA-N
LogP4.53
Synonyms
  • Fluroxypyr-meptyl
  • Octan-2-yl [(4-amino-3,5-dichloro-6-fluoropyridin-2-yl)oxy]acetate
  • Acetic acid, 2-[(4-amino-3,5-dichloro-6-fluoro-2-pyridinyl)oxy]-, 1-methylheptyl ester
  • 81406-37-3
  • Acetic acid, ((4-amino-3,5-dichloro-6-fluoro-2-pyridinyl)oxy)-, 1-methylheptyl ester
  • Fluroxypyr 1-methylheptyl ester
  • EINECS 279-752-9
  • Fluroxypyr-(1-methylheptyl)
  • Starane 250
  • Fluroxypyr meptyl

Applications:

HPLC Method for Analysis of Fluroxypyr-meptyl on Primesep 100 Column

May 18, 2023

HPLC Method for Separation of Fluroxypyr-meptyl on Primesep 100 by SIELC Technologies

Separation type: Liquid Chromatography Mixed-mode

HPLC Method for Analysis of Fluroxypyr-meptyl on Primesep 100 Column by SIELC Technologies

Fluroxypyr-meptyl is a herbicide used for the control of broad-leaved weeds in cereals, pastures, and non-crop areas. It belongs to a class of herbicides known as synthetic auxins.

Auxins are a class of plant hormones which are involved in the regulation of plant growth. Synthetic auxins like fluroxypyr mimic the action of natural auxins but disrupt the normal growth processes in the target plants, leading to their death.

Fluroxypyr-meptyl is effective against a range of weed species, including some that are resistant to other types of herbicides.

This herbicide can be retained and analyzed on a mixed-mode Primesep 100 column with a mobile phase consisting of water, Acetonitrile (MeCN), and Sulfuric acid (H2SO4). This analytical method can be UV detected at 220 nm with high resolution and peak symmetry.

LOD was determined for this combination of instrument, method, and analyte, and it can vary from one laboratory to another even when the same general type of analysis is being performed.

High Performance Liquid Chromatography (HPLC) Method for Analysis of Fluroxypyr-meptyl

Condition

ColumnPrimesep 100, 4.6 x 150 mm, 5 µm, 100 A
Mobile PhaseMeCN/H2O – 70/30%
BufferH2SO4 – 0.2%
Flow Rate1.0 ml/min
DetectionUV 220 nm
Peak Retention Time3.82 min
LOD0.1 ppm

Description

Class of CompoundsHerbicide
Analyzing CompoundsFluroxypyr-meptyl

Application Column

Primesep 100

Column Diameter: 4.6 mm
Column Length: 150 mm
Particle Size: 5 µm
Pore Size: 100 A

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Application Analytes:
Fluroxypyr-meptyl

Application Detection:
UV Detection
SIELC Technologies usually develops more than one method for each compound. Therefore, this particular method may not be the best available method from our portfolio for your specific application. Before you decide to implement this method in your research, please send us an email to research@sielc.com so we can ensure you get optimal results for your compound/s of interest.

Separation of Fluroxypyr-meptyl on Newcrom R1 HPLC column

February 16, 2018
Separation of Fluroxypyr-meptyl on Newcrom C18 HPLC column

Fluroxypyr-meptyl can be analyzed by this reverse phase (RP) HPLC method with simple conditions. The mobile phase contains an acetonitrile (MeCN), water, and phosphoric acid. For Mass-Spec (MS) compatible applications the phosphoric acid needs to be replaced with formic acid. Smaller 3 µm particles columns available for fast UPLC applications. This liquid chromatography method is scalable and can be used for isolation impurities in preparative separation. It also suitable for pharmacokinetics.

Application Column

Newcrom R1

The Newcrom columns are a family of reverse-phase-based columns. Newcrom A, AH, B, and BH are all mixed-mode columns with either positive or negative ion-pairing groups attached to either short (25 Å) or long (100 Å) ligand chains. Newcrom R1 is a special reverse-phase column with low silanol activity.

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Application Analytes:
Fluroxypyr-meptyl
The result was obtained by a proprietary SIELC algorithm. It may deviate from the actual experimental data. The experimental data are available upon request. Contact us by e-mail: support@sielc.com or by phone: 847-229-2629.