HPLC Method for Propranolol on Primesep 100 by SIELC Technologies
High Performance Liquid Chromatography (HPLC) Method for Analysis of Propranolol
Propranolol is an organic compound with the molecular formula C16H21NO2.
Properties:
Appearance: Typically a white or off-white crystalline powder
Molecular weight: ~259.34 g/mol
Solubility: Soluble in water and ethanol
Uses: Beta-blocker medication for cardiovascular and non-cardiovascular conditions
Propranolol can be retained and analyzed using the Primesep 100 stationary phase column. The analysis utilizes an isocratic method with a simple mobile phase consisting of water, acetonitrile (MeCN), and sulfuric acid. Detection is performed using UV at 270 nm.
Column | Primesep 100, 4.6 x 150 mm, 5 µm, 100 A, dual ended |
Mobile Phase | MeCN – 70% |
Buffer | H2SO4 – 0.1% |
Flow Rate | 1.0 ml/min |
Detection | UV 270 nm |
LOD | 14 ppb |
*LOD was determined for this combination of instrument, method, and analyte, and it can vary from one laboratory to another even when the same general type of analysis is being performed.
Class of Compounds | Synthetic Organic Compound |
Analyzing Compounds | Propranolol |
Application Column
Primesep 100
Column Diameter: 4.6 mm
Column Length: 150 mm
Particle Size: 5 µm
Pore Size: 100 A
Column options: dual ended